China Wholesale Electron Spin Resonance Factories – LADP-2 Experimental System of Pulsed NMR – Labor

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China Wholesale Electron Spin Resonance Factories – LADP-2 Experimental System of Pulsed NMR – Labor Detail:

Experiments

1. Understand the basic physical theory and experimental configuration of a PNMR system. Learn to explain related physical phenomena in PNMR using classical vector model.

2. Learn to use signals of spin echo (SE) and free induction decay (FID) to measure T₂ (spin-spin relaxation time). Analyze the influence of magnetic field homogeneity on NMR signal.

3. Learn to measure T₁ (spin-lattice relaxation time) using reverse recovery.

4. Qualitatively understand the relaxation mechanism, observe the effect of paramagnetic ions on nuclear relaxation time.

5. Measure T₂ of copper sulfate solution at different concentrations. Determine the relationship of T₂ with the change of concentration.

6. Measure the relative chemical displacement of the sample.

Specifications

Description	Specifications
Power supply of modulation field	maximum current 0.5 A, voltage regulation 0 – 6.00 V
Power supply of homogenous field	maximum current 0.5 A, voltage regulation 0 – 6.00 V
Oscillator frequency	20 MHz
Magnetic field strength	0.470 T
Magnetic pole diameter	100 mm
Magnetic pole distance	20 mm
Magnetic field homogeneity	20 ppm (10 mm × 10 mm × 10 mm)
Controlled temperature	36.500 °C
Magnetic field stability	4 hours warm to be stabilized, Larmor frequency drift less than 5 Hz per minute.

Parts List

Description	Qty	Note
Constant Temperature Unit	1	including magnet and temperature control device
RF Transmitting Unit	1	including power supply of modulation field
Signal Receiving Unit	1	including power supply of homogenous field and temperature display
Power Cord	1
Various Cable	12
Sample Tubes	10
Instructional Manual	1

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